Thermo-catalytic conversion is a pivotal process in the production of biofuels and bioenergy, involving the use of heat and catalysts to transform biomass into valuable energy carriers. This technique enhances the efficiency of converting organic materials into biofuels such as bio-oil, biodiesel, and biochar. During this process, biomass undergoes thermal decomposition in the presence of a catalyst, which accelerates chemical reactions and improves yield. The choice of catalyst and operational conditions, including temperature and pressure, significantly impact both the quality and quantity of the biofuels produced. By optimizing these parameters, thermo-catalytic conversion can produce cleaner, more efficient biofuels, contributing to a sustainable energy future and reducing reliance on fossil fuels.